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Synthesis and Characterization of a Bis(silyl) compound Based on O-Heterocyclic Aromatics

Corresponding Author : Rockshana Begum (rockshana-che@sust.edu)

Keywords : Silyl compounds, O-heterocyclic aromatic

Abstract :

A new bis(silyl) compound based on O-heterocyclic aromatics with the dibenzofuran backbone was prepared by dilithiation of the 4,5-positions of dibenzofuran using n-BuLi in the presence of tetramethylethylenediamine (TMEDA) followed by treatment with chlorodimethylsilane. The product DBFsil2 was characterized by 1H NMR, 13C NMR, 29Si NMR, Mass (EI) and Elemental analysis. 

Published on December 31st, 2012 in Volume 16, Issue 1, Applied Sciences and Technology